Latent Heat
Purpose:
To demonstrate the tremendous amount of energy released when
a liquid freezes to a solid.
Also to demonstrate the transformation of supercooled liquid to a
solid by nucleation on a seed.
Both are shown by analogy to the exothermic
crystallization of sodium acetate trihydrate from a
supersaturated solution of sodium acetate and water.
Procedure:
If flasks filled with solid sodium acetate
trihydrate are left from previous demonstrations (see TA office
cabinet), simply heat them to a boil until there is no solid left. It may be
necessary to add up to a tablespoon of water. Allow the flasks to
cool to room temperature before the demonstration.
If you have to make the solution, fill a flask 1 inch full with sodium
acetate trihydrate crystal and add enough water to wet crystals (about
a tablespoon). Heat to a boil until there is no solid left. Allow the
flasks to cool to room temperature before the demonstration.
Transport the flasks carefully so crystallization does not occur
prematurely.
Drop a few crystals of sodium acetate trihydrate into the flask to
provide a seed for crystallization. The solution solidifies
and the flask becomes toasty warm. Pass the flask around.
Equipment:
- Flask filled with a supersaturated solution of sodium acetate
trihydrate and water, stopper the flasks to keep the solution free of
impurities
- container of crystalline sodium acetate trihydrate
Comments:
The heat released is analogous to the latent heat
released in a phase transition. The mechanisms for releasing heat is
similar - a substantial change in the arrangement of molecules and
bonds when the phase transition (crystallization) occurs.
Some commercial hotpacks use this process.
References:
Contributors:
C. M. Bitz,
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